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Accepted Papers
The section containing accepted papers prior to their appearance in the forthcoming issues of Materials Science-Poland, is available on: Ahead of Print Articles.
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Effects of Ar+ ion sputtering on morphology and electric conductance of 6H-SiC (0001) surface
P. Mazur, S. Zuber, M. Grodzicki*, A. Ciszewski
Institute of Experimental Physics, University of Wroclaw, pl. Maxa Borna 9, 50-204 Wroclaw, Poland
Fabrication of micro- and nanostructures by scanning probe microscopy
local anodic oxidation
K. Kolanek1,*, T. Gotszalk1, M. Zielony1,
P. Grabiec2
1 Wrocław University of Technology, Faculty of Microsystem Electronics and Photonics, ul. Zygmunta Janiszewskiego 11/17, 50-372 Wroclaw, Poland
2 Institute of Electron Technology, Al. Lotników 32/46, 02-668 Warsaw, Poland
Surface nanomodification induced by neutralized ion beam
Z.W. Kowalski, J. Wilk
Wrocław University of Technology, Wybrzeże Wyspianskiego 27, 50-370 Wrocław, Poland
XPS study of air exposed CuPc ultra-thin films deposited on Si (111) native substrates
M. Krzywiecki1*, L. Grządziel1, L. Ottaviano2, P. Parisse2, S. Santucci2, J. Szuber1
1 Department of Electron Technology, Silesian University of Technology, 44-100 Gliwice,
Poland
2 Department of Physics, University of L'Aquila, I-67010 Coppito, Italy
Magnetic properties of ultrathin Co(0001) films on vicinal Si(111) substrate
A. Stupakiewicz1,2,*, A. Fleurence2, R. Gieniusz1,
A. Maziewski1, T. Maroutian2, P. Gogol2, B. Bartenlian2, R. Mégy2 and P. Beauvillain2
1Institute of Experimental Physics, University of Białystok, Lipowa 41,
15-424 Białystok, Poland
2Institut d'Electronique Fondamentale, Universite Paris XI; CNRS, UMR 8622,
F-91405 Orsay, France
Urea-urethane nanocomposites obtained from modified methylalumoxane oligomers
A. Boczkowska1*, M. Marczewski2, E. Ciecierska1, B. Sienkiewicz2 and
A. Pietrzykowski2
1Warsaw University of Technology, Faculty of Materials Science and Engineering, Woloska 141, 02-507 Warsaw, Poland
2 Warsaw University of Technology, Faculty of Chemistry, Noakowskiego 3, 00-664 Warsaw,
Poland
Aerosol-assisted synthesis of SiC-based nanopowders from organosilicon
precursor systems
C. Czosnek1*, S. Kluska2, J. F. Janik1
AGH University of Science and Technology, Al. Mickiewicza 30, 30-059 Kraków,
Poland;
1Faculty of Fuels and Energy,
2Faculty of Materials Science and Ceramics
Abstract
Thermally-driven decomposition of various organosilicon derivatives under a
neutral gas atmosphere constitutes a reliable way for the preparation of
carbon/silicon carbide C/SiC composites (modified carbon materials) in the
nanosized range. The two-stage aerosol-assisted synthesis method appears to be
especially well suited to make such materials while offering spherical particle
morphology with tailored particle size capability. In this method, in the first stage an
aerosol mist is generated from a liquid precursor system and transported in a neutral
gas stream to a pre-heated ceramic tube reactor where complex physical and
chemical changes take place resulting in the formation of solid particles that are
collected on an exit filter. This raw product is usually pyrolyzed in the second stage
at appropriately high temperatures to complete the anticipated removal of residual
oxygen if excess C is present via carbothermal reduction.
In this study, preliminary results on the target C/SiC composites prepared with
the aerosol method from selected organosilicon precursors are presented. The
precursors included hexamethyldisiloxane, tetramethoxysilane, and silicone oil
(poly(dimethylsiloxane)) and its ethanol solutions. In the first stage, the aerosols
were subjected to decomposition at 1200 ºC under an Ar flow and raw products
containing SiOxCy/SiO2 and free C of varied proportions were produced. In the second stage, the raw powders were pyrolyzed at 1650 ºC for 1 hour under an Ar
flow. The presence of sufficient excess of free C in the raw product should lead in
principle to efficient carbothermal reduction processes and conversion of SiOxCy/SiO2 to SiC in a composite system with the remaining free carbon, if any; otherwise, SiC/SiO2 or even SiC/SiO2/Si composites can be produced.
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Synthesis of ceria-based nanopowders suitable for manufacturing solid oxide electrolytes
M. Dudek*, M. Mróz, Ł. Zych, E. Drożdż-Cieśla
AGH-University of Science and Technology, Faculty of Materials Science and Ceramics
30-059 Cracow, Poland
Nano-metric Y2O3-TiO2-ZrO2 solid solution powders and their utilization in the synthesis of composite powders with TiB2 and TiC inclusions
N. Moskała*, J. Morgiel**, W. Pyda*
*AGH-University of Science and Technology, Faculty of Materials Science and Ceramics Department of Advances Ceramics, Al. Mickiewicza 30, 30-059 Cracow, Poland
** Institute of Metallurgy and Materials Science of the Polish Academy of Sciences ul. W. Reymonta 25, 30-059 Cracow, Poland
Titanium-ceramic nanocomposites prepared by mechanical alloying process
K. Niespodziana 1*, K. Jurczyk 2, M. Jurczyk1
1 Poznan University of Technology, Institute of Materials Science and Engineering,
Sklodowska-Curie 5 Sq., 60-965 Poznan, Poland
2 Poznan University of Medical Sciences, Department of Conservative Dentistry and
Periodontology, Bukowska 70 St., 60-812 Poznan, Poland
The influence of iron nanocrystallites size on nitriding process rate
R. Pelka*, P. Glinka, W. Arabczyk
Institute of Chemical and Environment Engineering, Szczecin University of Technology,
Pułaskiego 10, 70-322 Szczecin
Preparation of carbon encapsulated cobalt nanoparticles by catalytic ethane
decomposition
M. Podsiadły1*,U. Narkiewicz1, W. Arabczyk1,
M. J. Woźniak2, K.J. Kurzydłowski2
1 Institute of Chemical and Environment Engineering, Szczecin University of Technology, Pułaskiego 10, 70-322 Szczecin
2 Faculty of Materials Science and Engineering, Warsaw University of Technology,
141 Woloska Str., 02-507 Warsaw, Poland
Structure and properties of polyurethane nanocomposites modified by dibutylphosphate
boehmite
J. Ryszkowska, M. Jurczyk
Warsaw University of Technology,
Faculty of Materials Science and Engineering,
Woloska 141, 02-507 Warsaw, Poland
Structural and Textural Evolution of Zirconia Nanocrystals
Induced by Thermal Treatment
A. Adamski 1,*, P. Jakubus 2, Z. Sojka 1,3
1 Jagiellonian University, Faculty of Chemistry, Ingardena 3, PL 30-060 Cracow, Poland
2 Szczecin Technical University, Institute of Chemistry and Environment Protection,
al. Piastow 42, 71-065 Szczecin, Poland
3 Regional Laboratory of Physicochemical Analyses and Structural Research, Ingardena 3,
PL 30-060 Cracow, Poland
Nickel-free nanocrystalline austenitic stainless steels
Tulinski M.1, Jurczyk K. 2, Jurczyk M. 1
1 Poznan University of Technology, Institute of Materials Science and Engineering,
M. Sklodowska-Curie 5 Sq., 60-965 Poznań, Poland
2 Poznan University of Medical Sciences, Department of Conservative Dentistry and
Periodontology, Bukowska 70, 60-812 Poznań, Poland
Properties of films made from ZnS:Mn2+ nanoparticles.
A. Zdyb, K. Cieślak, J. M. Olchowik
Institute of Physics, Technical University of Lublin, ul. Nadbystrzycka 38 D
20-618 Lublin, Poland
Consolidation and sintering of nanometric ceramic powders
Ł. Zych
AGH - University of Science and Technology, Faculty of Materials Science and Ceramics,
al. Mickiewicza 30, 30-059 Krakow, Poland
Nano-ceramic Aspect of Preparation and Processing of the Zirconia Nano-powders
W. Pyda
AGH University of Science and Technology, Faculty of Materials Science and Ceramics,
Al. Mickiewicza, 30-059 Kraków
Iron filled carbon nanotubes for bio-applications
E. Borowiak-Palen
Szczecin University of Technology, Centre of Knowledge Based Technologies and Nanomaterials, Institute of
Chemical and Environment Engineering, Poland
Synthesis of silver nanoparticles using microorganisms
Zygmunt Sadowski, Irena Helena Maliszewska, Barbara Grochowalska,
I. Polowczyk, T. Koźlecki
Faculty of Chemistry, Wroclaw University of Technology
Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland
Nanosorbents for selective removal of odours
M. Ziolek, I. Sobczak, A. Dudzik,Ł. Konwicki, J. Kujawa
Adam Mickiewicz University, Faculty of Chemistry, ul. Grunwaldzka 6, 60-780 Poznań
Characterization of Carbon Nanotubes by Raman spectroscopy
S. Costa, E. Borowiak-Palen*, M. Kruszyńska, A. Bachmatiuk, R J. Kalenczuk
Centre of Knowledge Based Nanomaterials and Technologies, Institute of Chemical and
Environment Engineering, Szczecin University of Technology, Poland
Studies on biocompatible nanocapsules formed from microemulsion
templated processes
K. Zielińska1, K. A. Wilk1*, E. Seweryn2,
J. Saczko2, J. Pietkiewicz2
1 Department of Chemistry, Wroclaw University of Technology,
Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland
2Department of Medical Biochemistry, Medical University of Wroclaw,
Chałubińskiego 10, 50-368 Wrocław, Poland
The detection of some chloroorganic compounds by a microbial sensor system
I. Maliszewska, K. A. Wilk
Faculty of Chemistry, Wroclaw University of Technology
Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland
Ultrafiltration as a method of natural organic matter separation from water
M. Kabsch-Korbutowicz
Wrocław University of Technology,
Institute of Environment Protection Engineering,
Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland
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